课程信息
4.6
152 个评分
43 个审阅
100% 在线

100% 在线

立即开始,按照自己的计划学习。
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中级

中级

完成时间(小时)

完成时间大约为12 小时

建议:6 hours/week...
可选语言

英语(English)

字幕:英语(English)
100% 在线

100% 在线

立即开始,按照自己的计划学习。
可灵活调整截止日期

可灵活调整截止日期

根据您的日程表重置截止日期。
中级

中级

完成时间(小时)

完成时间大约为12 小时

建议:6 hours/week...
可选语言

英语(English)

字幕:英语(English)

教学大纲 - 您将从这门课程中学到什么

1
完成时间(小时)
完成时间为 3 小时

Ultraviolet and Visible Spectroscopy

In this first week we introduce the electromagnetic spectrum and the origin of transitions giving rise to ultraviolet and visible (UV/Vis) spectra. You will learn that electronic transitions are caused by absorption of radiation in the UV/Vis region of the electromagnetic spectrum. The reason for the wavelength and intensity of bands will be described and the colour origin of certain compounds will be discussed. You will also be shown how UV/Vis spectroscopy is performed and you will be able to run and analyse your own spectra. As the final activity in this module you are given a link to view how to obtain a UV/Visible spectrum in the laboratory. Good luck, try and participate in the discussion forums to enhance your learning and don't forget to complete the end of week laboratory quiz which contributes to your final mark....
Reading
10 个视频 (总计 89 分钟), 7 个阅读材料, 2 个测验
Video10 个视频
What is spectroscopy?9分钟
The nature and properties of electromagnetic radiation6分钟
Example of energy calculation10分钟
Energy levels: Molecular Orbital Theory - revision11分钟
Molecular Orbital diagram for CO5分钟
UV/Visible spectroscopy10分钟
Example of Beer-Lambert calculation8分钟
Transitions relevant to UV/Vis Spectroscopy15分钟
Effect of conjugation on wavelength8分钟
Reading7 个阅读材料
Guidance for studying the course10分钟
ACKNOWLEDGEMENTS10分钟
Pre-course survey5分钟
Week 1 Lecture Notes10分钟
Lab 1 Introduction10分钟
How to obtain a UV/Vis spectrum10分钟
Run a UV/Visible spectrum10分钟
Quiz2 个练习
Week 128分钟
UV/Vis laboratory quiz4分钟
2
完成时间(小时)
完成时间为 2 小时

Infrared Spectroscopy

In this module we introduce the theory underpinning infrared (IR) spectroscopy and show examples of analysis using the technique. Transitions between the vibrational energy levels of molecules occurs in the infrared region of the electromagnetic spectrum. We start with the theory underlying vibration using the simple harmonic oscillator model. Analysis of more complex molecules is introduced using group frequencies and number of vibrational modes. You will also be shown how to obtain an infrared spectrum and will have an opportunity to run your own spectrum. At the end of this module you are given a link to view how to obtain an infra red spectrum in the laboratory. Don't forget to complete the end of week laboratory quiz which contributes to your final mark for this course....
Reading
6 个视频 (总计 72 分钟), 4 个阅读材料, 2 个测验
Video6 个视频
Vibrational frequency12分钟
Example vibrational frequency calculation10分钟
Energy levels and dipoles14分钟
Vibrational modes9分钟
Example IR spectra of organic molecules12分钟
Reading4 个阅读材料
Week 2 Lecture Notes10分钟
Lab 2 Introduction10分钟
How to obtain an infra red spectrum10分钟
Run an infra red spectrum10分钟
Quiz2 个练习
Week 220分钟
IR Lab Quiz4分钟
3
完成时间(小时)
完成时间为 3 小时

Nuclear Magnetic Resonance (NMR) Spectroscopy

This week we concentrate on Nuclear Magnetic Resonance (NMR) spectroscopy. Here a magnetic field is used to create energy levels for magnetic nuclei present in a molecule. Transition between these energy levels occurs in the radiofrequency region of the electromagnetic spectrum. The positions of the bands in the observed spectrum is dependent on the shielding of the nuclei by the local electronic structure, giving rise to a parameter known as chemical shift. Bands also display fine structure caused by spin-spin coupling with neighbouring nuclei. Examples on the analysis of NMR spectra for structure determination will be given. As the final activity in this module you are given a link to view how to obtain an NMR spectrum in the laboratory. Don't forget to compete this end of week laboratory quiz which contributes to your final mark. ...
Reading
9 个视频 (总计 114 分钟), 4 个阅读材料, 2 个测验
Video9 个视频
Nuclear spin in an external magnetic field10分钟
Spin and magnetisation13分钟
Chemical shift18分钟
More on chemical shift19分钟
Analysis of proton spectra5分钟
Spin-spin coupling6分钟
Spin-spin coupling mechanism18分钟
Carbon-13 NMR and pulsed methods10分钟
Reading4 个阅读材料
Week 3 Lecture Notes10分钟
Lab 3 Introduction10分钟
How to obtain an NMR spectrum10分钟
Run an NMR spectrum10分钟
Quiz2 个练习
Week 320分钟
NMR lab quiz4分钟
4
完成时间(小时)
完成时间为 1 小时

Final Assessment

...
Reading
1 个测验
Quiz1 个练习
Week 4 Quizs
4.6
43 个审阅Chevron Right

热门审阅

创建者 ESApr 3rd 2018

Excellent material and pace. Assignments were challenging but could be completed from the lecture material alone. Overall a great experience.

创建者 JLAug 26th 2018

Very recommended to every person who wants to understand the basic ideas, concepts and calculations of current spectroscopic techniques.

讲师

关于 University of Manchester

Tracing its roots back to 1824, the University of Manchester is home to almost 40,000 students. The University has three Nobel laureates among its current staff – more than any other British university - and a total of 25 Nobel laureates have come from our past and present students and staff. We have three main goals: to undertake world-class research; to deliver an outstanding learning and student experience; and to be socially responsible....

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